Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation

Fritz Duus; Nhuan Ngoc Doan; Thach Ngoc Le; Poul Erik Hansen

Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation

Fritz Duus
, Nhuan Ngoc Doan
, Thach Ngoc Le
, Poul Erik Hansen

Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › peer review

Abstract

Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.

Originalsprog	Engelsk
Tidsskrift	Tetrahedron Letters
Vol/bind	46
Sider (fra-til)	6749-6751
Antal sider	3
ISSN	0040-4039
Status	Udgivet - 2005

Citationsformater

@article{37c4217052cf11db8236000ea68e967b,

title = "Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation",

abstract = "Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.",

author = "Fritz Duus and Doan, \{Nhuan Ngoc\} and Le, \{Thach Ngoc\} and Hansen, \{Poul Erik\}",

year = "2005",

language = "English",

volume = "46",

pages = "6749--6751",

journal = "Tetrahedron Letters",

issn = "0040-4039",

publisher = "Pergamon Press",

}

TY - JOUR

T1 - Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation

AU - Duus, Fritz

AU - Doan, Nhuan Ngoc

AU - Le, Thach Ngoc

AU - Hansen, Poul Erik

PY - 2005

Y1 - 2005

N2 - Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.

AB - Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.

M3 - Journal article

SN - 0040-4039

VL - 46

SP - 6749

EP - 6751

JO - Tetrahedron Letters

JF - Tetrahedron Letters

ER -