Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation

Fritz Duus, Nhuan Ngoc Doan, Thach Ngoc Le, Poul Erik Hansen

    Publikation: Bidrag til tidsskriftTidsskriftartikelForskningpeer review

    Resumé

    Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.
    OriginalsprogEngelsk
    TidsskriftTetrahedron Letters
    Vol/bind46
    Sider (fra-til)6749-6751
    Antal sider3
    ISSN0040-4039
    StatusUdgivet - 2005

    Citer dette

    @article{37c4217052cf11db8236000ea68e967b,
    title = "Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation",
    abstract = "Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.",
    author = "Fritz Duus and Doan, {Nhuan Ngoc} and Le, {Thach Ngoc} and Hansen, {Poul Erik}",
    year = "2005",
    language = "English",
    volume = "46",
    pages = "6749--6751",
    journal = "Tetrahedron Letters",
    issn = "0040-4039",
    publisher = "Pergamon Press",

    }

    Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation. / Duus, Fritz; Doan, Nhuan Ngoc; Le, Thach Ngoc; Hansen, Poul Erik.

    I: Tetrahedron Letters, Bind 46, 2005, s. 6749-6751.

    Publikation: Bidrag til tidsskriftTidsskriftartikelForskningpeer review

    TY - JOUR

    T1 - Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation

    AU - Duus, Fritz

    AU - Doan, Nhuan Ngoc

    AU - Le, Thach Ngoc

    AU - Hansen, Poul Erik

    PY - 2005

    Y1 - 2005

    N2 - Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.

    AB - Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluene-sulfonic acid on silica gel under solventless conditions.

    M3 - Journal article

    VL - 46

    SP - 6749

    EP - 6751

    JO - Tetrahedron Letters

    JF - Tetrahedron Letters

    SN - 0040-4039

    ER -