A natural abundance 15N NMR investigation of bilirubin IX‐α

Poul E. Hansen; Hans J. Jakobsen

doi:10.1002/mrc.1270221015

A natural abundance ¹⁵N NMR investigation of bilirubin IX‐α

Poul E. Hansen
, Hans J. Jakobsen^*

^*Corresponding author

Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › peer review

7 Citationer (Scopus)

Abstract

Natural abundance 15N NMR spectra have been obtained for bilirubin IX‐α using polarization transfer via the INEPT and SINEPT‐2 techniques. The resonances for all four nitrogens are clearly resolved. 15N chemical shifts and 15N1H coupling constants over one and three bonds are reported. Heteronuclear chemical shift correlation between 15N and 1H for the four NH groups has been established by means of the SINEPT‐2 pulse sequence.

Originalsprog	Engelsk
Tidsskrift	Organic Magnetic Resonance
Vol/bind	22
Udgave nummer	10
Sider (fra-til)	668-670
Antal sider	3
ISSN	0030-4921
DOI	https://doi.org/10.1002/mrc.1270221015
Status	Udgivet - okt. 1984

Adgang til dokumentet

10.1002/mrc.1270221015

Citationsformater

@article{d7b64e1e9eee4c0681b42e462b4aca6b,

title = "A natural abundance 15N NMR investigation of bilirubin IX‐α",

abstract = "Natural abundance 15N NMR spectra have been obtained for bilirubin IX‐α using polarization transfer via the INEPT and SINEPT‐2 techniques. The resonances for all four nitrogens are clearly resolved. 15N chemical shifts and 15N1H coupling constants over one and three bonds are reported. Heteronuclear chemical shift correlation between 15N and 1H for the four NH groups has been established by means of the SINEPT‐2 pulse sequence.",

author = "Hansen, \{Poul E.\} and Jakobsen, \{Hans J.\}",

year = "1984",

month = oct,

doi = "10.1002/mrc.1270221015",

language = "English",

volume = "22",

pages = "668--670",

journal = "Organic Magnetic Resonance",

issn = "0030-4921",

publisher = "JohnWiley \& Sons Ltd.",

number = "10",

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TY - JOUR

T1 - A natural abundance 15N NMR investigation of bilirubin IX‐α

AU - Hansen, Poul E.

AU - Jakobsen, Hans J.

PY - 1984/10

Y1 - 1984/10

N2 - Natural abundance 15N NMR spectra have been obtained for bilirubin IX‐α using polarization transfer via the INEPT and SINEPT‐2 techniques. The resonances for all four nitrogens are clearly resolved. 15N chemical shifts and 15N1H coupling constants over one and three bonds are reported. Heteronuclear chemical shift correlation between 15N and 1H for the four NH groups has been established by means of the SINEPT‐2 pulse sequence.

AB - Natural abundance 15N NMR spectra have been obtained for bilirubin IX‐α using polarization transfer via the INEPT and SINEPT‐2 techniques. The resonances for all four nitrogens are clearly resolved. 15N chemical shifts and 15N1H coupling constants over one and three bonds are reported. Heteronuclear chemical shift correlation between 15N and 1H for the four NH groups has been established by means of the SINEPT‐2 pulse sequence.

U2 - 10.1002/mrc.1270221015

DO - 10.1002/mrc.1270221015

M3 - Journal article

AN - SCOPUS:84986848636

SN - 0030-4921

VL - 22

SP - 668

EP - 670

JO - Organic Magnetic Resonance

JF - Organic Magnetic Resonance

IS - 10

ER -